CEMS

Industrial Collaborators, Both Past and Present


Industrial collaborators are an important part of our research, because of the genuine intellectual collaboration as well as their financial support. With the reduction in industrial research that has been and is continuing in the chemical industry, I believe that research done in a University setting offers many advantages to a corporation. Chief among these advantages is the incredibly low cost of sponsoring programs at a University along with the cutting edge equipment and high level of fundamental understanding available at a University. Corporations have sponsored over $1,000,000 worth of research in our group. The companies listed below that have sponsored our research with funds; other companies such as Solvay and ExxonMobil have donated polymers for use in our laboratories. A brief description of a selected number of different projects is given below so that the reader can truly understand the wide variety of industrial projects in our laboratory.

Development of A Nano-Coating for Dental Implants sponsored by Imtec
Poly lactic-co-glycolic (PLGA) nanoparticles are well-known for their ability to degrade and release pharmaceutics. Our group is taking this approach a bit further. We are developing ~300 nm nanoparticles with encapsulated ~20 nm hydroxyapatite nanoparticles (hydroxyapatite is very similar to bone) in order to speed healing of dental implants. Dental implants are screwed into the jawbone and provide an excellent way to permanently replace missing teeth; however one disadvantage is that the time to full functionality is ~6 months. Our goal is to speed this healing time. This project is being done in collaboration with Dr. Vassilios Sikavitsas.

Development of A Method to Increase Fracture Stress of Rock in Oil Wells sponsored by Halliburton
The layer-by-layer method is a well-known method for "growing" a polymer film on a surface. The principle is to use charged polymers to adsorb to an oppositely charged surface, then grow the layers sequentially by alternating polymers having different charge. The same principle is used here, except latex beads are used. One can build up a layer using this technique, which in turn increases the hydrostatic stress required to crack the rock.

Development of A Replacement for Portland Cement for Use in Oil Wells sponsored by Halliburton
Low-cost polyalkenoate cements analogous to dental cements, i.e. cements based on polymers containing acrylic acid crosslinked both covalently and via bridging metal cations, were developed with a goal of producing a more flexible alternative to normal Portland cement. This project was very successful, and resulted in a patent application that should eventually become a patent.

Development of Modified Sand sponsored by Halliburton
We are attempting to modify the surface of sand in order to improve the ability of this material to function well in an oil well. Sand is used to keep cracks open in the ground so that oil can seep out from the surrounding rock and eventually make its way to the surface. The sand reaches the crack via suspension in a polymer-water mixture and flow of the water to the crack, and once in place the oil flows through the sand. Hence the important properties of the sand are its ability to remain suspended in the polymer-water mixture and its conductivity of oil through the pores of the packed sand.

X-ray Absorption Spectroscopy of Surlyn Ionomers sponsored by DuPont (Sabine Research Laboratory)
Surlyn ion-containing polymers are copolymers of ethylene and methacrylic acid. Our purpose is to understand on a molecular basis why ionomers have such interesting properties, such as why they are so incredibly tough. Our approach is to quantify arrangement of atoms, i.e. what atoms are located where, using EXAFS. Our unique capabilities led to a National Science Foundation sponsored program to research these materials, as well as significant direct financial and material support by DuPont. The ionomer page gives a list of the publications that was the result of support of this research.

Powder Coating Product Support sponsored by Innotek Powder Coatings LLC
Our interaction with PFS has been in the area of product development and product characterization. PFS produces thermoplastic powders and powder coating equipment for a wide variety of customers. Powder coating with thermoplastics consists of taking a thermoplastic material, grinding it to make a powder, then coating the object either by flame-spraying, electrostatic spraying or dip coating. The primary use of powder coating is for corrosion protection, although there are many other uses as well. Our laboratory has developed a proprietary method to characterize the rheology of the powder coating process, and has used this process to identify materials that are good candidates for product development as a powder coating.

Interaction of Surface Treatments using Water-Based Cleaners with Different Coatings sponsored by Chemical Process Industries
CPI is a small Oklahoma City based corporation. CPI manufactures and sells a water-based cleaner to be used for cleaning surfaces prior to coating under the AquaCleen trademark. In our laboratory, we evaluate how different formulations of this cleaner interact with off the shelf paints and other coatings on different surfaces. The evaluation process includes detailed statistical measures of any changes in performance, and fundamental investigations of what causes the interations.


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